HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → HCID 14003461, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Ethyl alpha-oxobenzenebutanoate | HCID 562087 | — |
| Reactant | HCID 14003453 | HCID 14003453 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14003461 | HCID 14003461 | — |
Reaction Steps
A solution of 3.8 g of this amine, 3.7 g ethyl 2-oxo-4-phenylbutyrate and 0.68 ml acetic acid in 50 ml ethanol is hydrogenated and the isomers separated as described in Example 27 to afford 1-t-butoxycarbonylmethyl-3-(1-ethoxycarbonyl-3-phenylpropyl)amino-7-phenylperhydroazepin-2-one:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04629787 |
| Source dataset | uspto-grants-1986_12 |
| ORD ID | ord-55b7c95589d346839eae7dfbf4509b41 |
| Source note | uspto-grants-1986_12 |