3-Cyano-4,6-dimethyl-2-hydroxypyridine → HCID 11805265, compound

HRID 1249318Notes

Reaction equation

HRID 1249318 reaction equation
[C:1]([C:3]1[C:4](=[O:11])[NH:5][C:6]([CH3:10])=[CH:7][C:8]=1[CH3:9])#[N:2].F[B-](F)(F)F.[CH2:17]([O+](CC)CC)[CH3:18]>ClCCl>[C:1]([C:3]1[C:4]([O:11][CH2:17][CH3:18])=[N:5][C:6]([CH3:10])=[CH:7][C:8]=1[CH3:9])#[N:2]

Participants

4

Reactant 2

HCID 698563-Cyano-4,6-dimethyl-2-hydroxypyridineHCID 2723982Triethyloxonium tetrafluoroborate

Product 1

HCID 11805265HCID 11805265, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

3-Cyano-2-ethoxy-4,6-dimethylpyridine was prepared by reacting 3-cyano-4,6-dimethylpyrid-2-one with triethyloxonium tetrafluoroborate in dichloromethane.

Sources & evidence

ORD record
ord-a85d92ba44e14bfabfadf1ca89e274f0
Source dataset
uspto-grants-1986_12
Patent number
US04631081

Reaction notes

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