Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1) → HCID 13590770, compound

HRID 1249348Notes

Reaction equation

HRID 1249348 reaction equation
[CH3:1][O:2][C:3]1[C:8]2[O:9][CH:10]3[CH2:16][CH2:15][CH2:14][CH:13]([OH:17])[CH:11]3[O:12][C:7]=2[CH:6]=[CH:5][CH:4]=1.Cl.Cl[CH2:20][CH2:21][N:22]1[CH2:27][CH2:26][O:25][CH2:24][CH2:23]1>>[O:25]1[CH2:26][CH2:27][N:22]([CH2:21][CH2:20][O:17][CH:13]2[CH:11]3[O:12][C:7]4[CH:6]=[CH:5][CH:4]=[C:3]([O:2][CH3:1])[C:8]=4[O:9][CH:10]3[CH2:16][CH2:15][CH2:14]2)[CH2:23][CH2:24]1

Participants

3

Reactant 2

HCID 77210Morpholine, 4-(2-chloroethyl)-, hydrochloride (1:1)HCID 13590768HCID 13590768, compound

Product 1

HCID 13590770HCID 13590770, compoundYield 55.7%

Procedure

In an analogous manner as described in Example 3, but starting with 10 g (0.042 mole) of the alcohol of Example 2 and 9 g (0.038 mole) of 4-(2-chloroethyl)morpholine hydrochloride, there were obtained 7.4 g of the title-compound of boiling point 192°-195° C. at a pressure of 65 Pa, having the elementary analysis:

Sources & evidence

ORD record
ord-0f9541c68c4f4261856bd32b98c41349
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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