2-Chloroethyldiisopropylammonium chloride → HCID 13590771, compound

HRID 1249349Notes

Reaction equation

HRID 1249349 reaction equation
[CH2:1]1[CH:10]2[CH:5]([O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9]2)[CH:4]([OH:15])[CH2:3][CH2:2]1.Cl.Cl[CH2:18][CH2:19][N:20]([CH:24]([CH3:26])[CH3:25])[CH:21]([CH3:23])[CH3:22]>>[CH:21]([N:20]([CH:24]([CH3:26])[CH3:25])[CH2:19][CH2:18][O:15][CH:4]1[CH:5]2[O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9][CH:10]2[CH2:1][CH2:2][CH2:3]1)([CH3:23])[CH3:22]

Participants

3

Reactant 2

HCID 779422-Chloroethyldiisopropylammonium chlorideHCID 13590767HCID 13590767, compound

Product 1

HCID 13590771HCID 13590771, compoundYield 82.2%

Procedure

Working as described in Example 3, but starting with 12.4 g (0.06 mole) of the alcohol of Example 1 and 10 g (0.05 mole) of 1-chloro-2-diisopropylaminoethane hydrochloride, there were obtained 13.7 g of the title-compound of melting point 63.4° C., having the elementary analysis:

Sources & evidence

ORD record
ord-9433952a6bde4447a52cf5f79d9540bc
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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