3-(Dimethylamino)propyl chloride hydrochloride → HCID 13590772, compound

HRID 1249350Notes

Reaction equation

HRID 1249350 reaction equation
[CH2:1]1[CH:10]2[CH:5]([O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9]2)[CH:4]([OH:15])[CH2:3][CH2:2]1.Cl.[CH3:17][N:18]([CH3:23])[CH2:19][CH2:20][CH2:21]Cl>>[CH3:17][N:18]([CH3:23])[CH2:19][CH2:20][CH2:21][O:15][CH:4]1[CH:5]2[O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9][CH:10]2[CH2:1][CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 943083-(Dimethylamino)propyl chloride hydrochlorideHCID 13590767HCID 13590767, compound

Product 1

HCID 13590772HCID 13590772, compoundYield 55.6%

Procedure

In an analogous manner as described in Example 5, but starting with 10 g (0.048 mole) of the alcohol of Example 1 and 6.6 g (0.042 mole) of 3-dimethylamino-1-chloropropane hydrochloride, there were obtained 6.8 g of the title-compound of boiling point 165° C. at a pressure of 1.33 Pa, having the elementary analysis:

Sources & evidence

ORD record
ord-cfeaa6bc34314fe7a1763498cdcc6d85
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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