HCID 12794507, compound → HCID 13590773, compound

HRID 1249351Notes

Reaction equation

HRID 1249351 reaction equation
[CH2:1]1[CH:10]2[CH:5]([O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9]2)[CH:4]([OH:15])[CH2:3][CH2:2]1.Cl.Cl[CH2:18][C:19]([CH3:25])([CH3:24])[CH2:20][N:21]([CH3:23])[CH3:22]>>[CH3:18][C:19]([CH3:25])([CH2:20][N:21]([CH3:23])[CH3:22])[CH2:24][O:15][CH:4]1[CH:5]2[O:6][C:7]3[CH:14]=[CH:13][CH:12]=[CH:11][C:8]=3[O:9][CH:10]2[CH2:1][CH2:2][CH2:3]1

Participants

3

Reactant 2

HCID 12794507HCID 12794507, compoundHCID 13590767HCID 13590767, compound

Product 1

HCID 13590773HCID 13590773, compoundYield 58.5%

Procedure

In an analogous manner as described in Example 5, but starting with 10 g (0.048 mole) of the alcohol of Example 1 and 8.6 g (0.046 mole) of 1-chloro-2,2-dimethyl-3-dimethylaminopropane hydrochloride, there were obtained 8.6 g of the title-compound of boiling point 135° C. at a pressure of 6.5 Pa, having the elementary analysis:

Sources & evidence

ORD record
ord-cd3ec3bdf81a41b2b96ff1b95fbd9c34
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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