Methyl Bromide → HCID 13590774, compound

Participants

Reaction Steps

In an autoclave, 900 g (2.82 moles) of the amino ether of Example 3 were dissolved in 3 liters of acetone, and 535.6 g (5.64 moles) of methyl bromide were added. After crystallisation had started, the mixture was left with stirring for 2 hours at room temperature. After being filtered and rinsed with acetone, the solid formed was resuspended in petroleum ether, stirring, filtered, dried under vacuum and then recrystallised in a minimum quantity of the mixture diisopropyl ether/isopropanol (7:3). There were thus obtained 1000 g of the title-compound of melting point 155° C., having the elementary analysis:

Provenance & Evidence