Methyl iodide → HCID 20224487, compound

HRID 1249354Notes

Reaction equation

HRID 1249354 reaction equation
[O:1]1[CH2:6][CH2:5][N:4]([CH2:7][CH2:8][O:9][CH:10]2[CH:15]3[O:16][C:17]4[CH:23]=[CH:22][CH:21]=[CH:20][C:18]=4[O:19][CH:14]3[CH2:13][CH2:12][CH2:11]2)[CH2:3][CH2:2]1.[CH3:24][I:25]>>[I-:25].[CH2:13]1[CH:14]2[CH:15]([O:16][C:17]3[CH:23]=[CH:22][CH:21]=[CH:20][C:18]=3[O:19]2)[CH:10]([O:9][CH2:8][CH2:7][N+:4]2([CH3:24])[CH2:3][CH2:2][O:1][CH2:6][CH2:5]2)[CH2:11][CH2:12]1

Participants

3

Reactant 2

HCID 6328Methyl iodideHCID 13590769HCID 13590769, compound

Product 1

HCID 20224487HCID 20224487, compoundYield 64.7%

Procedure

In an analogous manner as described in Example 8 but starting with 600 g (1.88 moles) of the compound of Example 3 and 537.4 g (3.76 moles) of methyliodide, there were obtained 561 g of the title-compound with melting point 162° C.

Sources & evidence

ORD record
ord-332e9703b42a405693060b234354b2c4
Source dataset
uspto-grants-1986_12
Patent number
US04631277

Reaction notes

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