HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53962035, compound → 1H-Indole-2-carboxylic acid, 4-chloro-, Methyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53962035 | HCID 53962035 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1H-Indole-2-carboxylic acid, 4-chloro-, Methyl ester | HCID 4714974 | — |
Reaction Steps
Methyl 2-azido-3-(2-chlorophenyl)-propenoate (3.566 g, 144 mmol) was suspended in toluene (800 ml) and the mixture was heated at reflux for three hours, then cooled and allowed to stir at room temperature overnight. A yellow crystalline material was obtained by filtration and recrystallised from hexane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06335360B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-9fbec446f6ef4eada94f1b9e25d08cbe |
| Source note | uspto-grants-2002_01 |