HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22983849, compound → HCID 22983844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22983849 | HCID 22983849 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 22983844 | HCID 22983844 | 72.2% |
Reaction Steps
3-O-benzyl-1,2-di-O-eicosyl-Sn-glycerol (1.47 g, 1.98 mmol) and 10% palladium-charcoal (200 mg) were stirred in ethyl acetate (30 ml) under the hydrogen atmosphere at room temperature for 18 h. The reaction mixture was filtered through celite, and the filtrate was concentrated in vacuo to obtain the title compound (934 mg, 72%) as white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337390B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-f3f1e70d45dd4cf79805e053d96ea377 |
| Source note | uspto-grants-2002_01 |