Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | HCID 22601176 | HCID 22601176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 22601167 | HCID 22601167 | 98.1% |
Reaction Steps
After a mixture of 2,2-bis(docosyloxymethyl)propyl methanesulfonate (22.7 g; 27.8 mmol), sodium azide (0.27 g; 83.5 mmol), and dimethylformamide (150 ml) was stirred at 110° C. for 20 h, the reaction mixture was poured into water. Precipitates thus obtained were collected by suction, washed successively with water and acetone, and dried to obtain the title compound (20.8 g; 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06337390B1 |
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| Source dataset | uspto-grants-2002_01 |
|---|
| ORD ID | ord-e680a0188178482cbf9e17e7833b5bbb |
|---|
| Source note | uspto-grants-2002_01 |
|---|
