HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 18327971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 18328033 | HCID 18328033 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18327971 | HCID 18327971 | — |
Reaction Steps
1.56 g of the compound of step 1 of Example 29 was dissolved in 15 ml of pyridine, 0.8 ml (1.5 equivalents) of phosphorus oxychloride was added under ice cooling and the result was agitated for 16 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06337397B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-a6c26797fb7c47a5be188b7db05d7eb8 |
| Source note | uspto-grants-2002_01 |