HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → [(4-Bromophenyl)methyl]triphenylphosphanium bromide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | [(4-Bromophenyl)methyl]triphenylphosphanium bromide | HCID 2724858 | 95% |
Reaction Steps
Triphenylphosphine and benzene were added to 4-bromobenzyl bromide, and then the mixture was refluxed for 12 hours, resulting in 4-bromobenzyltriphenylphosphonium bromide (G) (yield: 95%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06338909B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-107f6f2091104d64a278e57715841847 |
| Source note | uspto-grants-2002_01 |