HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzyl bromide → Methyl 4-(4-bromobenzylamino)-2,5-dimethylquinoline-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzyl bromide | HCID 68527 | — |
| Reactant | 1-(4-(4-Bromobenzylamino)-2-methylquinolin-3-yl)ethanone | HCID 11462804 | — |
| Reactant | Methyl 4-amino-2,5-dimethylquinoline-3-carboxylate | HCID 18326317 | — |
| Product | Methyl 4-(4-bromobenzylamino)-2,5-dimethylquinoline-3-carboxylate | HCID 12019300 | — |
Reaction Steps
Methyl 4-(4-bromobenzylamino)-2,5-dimethylquinoline-3-carboxylate was synthesized by the same process as described for 1-(4-(4-bromobenzylamino)-2-methylquinolin-3-yl)ethanone (Example 1, Intermediate 2c) starting from methyl 4-amino-2,5-dimethylquinoline-3-carboxylate and 4-bromobenzyl bromide. Melting point: 150° C.; MS(Cl+): 399/401.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06339077B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-9dcc46fce9594c35af1cf23bac78222a |
| Source note | uspto-grants-2002_01 |