4-Bromobenzylamine → HCID 12019328, compound
Reaction equation
[Br:1][C:2]1[CH:23]=[CH:22][C:5]([CH2:6][NH:7][C:8]2[C:17]3[C:12](=[CH:13][CH:14]=CC=3)[N:11]=[C:10]([CH3:18])[C:9]=2[C:19](=[O:21])[CH3:20])=[CH:4][CH:3]=1.ClC1C=C(C)N=C(CC)C=1.BrC1C=CC(CN)=CC=1>>[Br:1][C:2]1[CH:23]=[CH:22][C:5]([CH2:6][NH:7][C:8]2[C:9]([C:19](=[O:21])[CH3:20])=[C:10]([CH3:18])[N:11]=[C:12]([CH2:13][CH3:14])[CH:17]=2)=[CH:4][CH:3]=1Participants
4
Procedure
1-[4-(4-Bromobenzylamino)-2-ethyl-6-methylpyridin-5-yl]ethanone was prepared by the method described in Example 30 (Intermediate 2c) starting from 4-chloro-2-ethyl-6-methylpyridine and 4-bromobenzylamine. MS(ES+): 347/349.
Sources & evidence
- ORD record
- ord-969caff4648c4f75bfd9d039fb06aaca
- Source dataset
- uspto-grants-2002_01
- Patent number
- US06339077B1
Reaction notes
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