HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → 2-Allylamino-4-dodecylamino-6-nitroquinazoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | 2-Chloro-4-dodecylamino-6-nitroquinazoline | HCID 18326516 | — |
| Solvent | Water | HCID 962 | — |
| Product | 2-Allylamino-4-dodecylamino-6-nitroquinazoline | HCID 18326548 | 93.4% |
Reaction Steps
To 170 mg (0.44 mmol) of 2-chloro-4-dodecylamino-6-nitroquinazoline was added 1.70 ml (22.66 mmol) of allylamine, and then the resulting mixture was stirred at room temperature overnight. After water was added to the reaction solution, crystals thus precipitated were filtered to give 170 mg (93.4%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06339089B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-46e3260cc7e241ce9c3303d32471a74b |
| Source note | uspto-grants-2002_01 |