HCID 18324905, compound → HCID 9865453, compound

HRID 1250911Notes

Reaction equation

HRID 1250911 reaction equation
[F:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([C:11]3[CH:16]=[CH:15][C:14]([S:17]([CH3:20])(=[O:19])=[O:18])=[CH:13][CH:12]=3)=[C:8](I)[C:7](=[O:22])[C:6]=2[CH:23]=1.CO[C:26]1[C:27](OC)=[C:28](B([O-])[O-])[C:29](OC)=[N:30][CH:31]=1.[Li+].[Li+]>>[F:1][C:2]1[CH:3]=[CH:4][C:5]2[O:10][C:9]([C:11]3[CH:16]=[CH:15][C:14]([S:17]([CH3:20])(=[O:19])=[O:18])=[CH:13][CH:12]=3)=[C:8]([C:28]3[CH:29]=[N:30][CH:31]=[CH:26][CH:27]=3)[C:7](=[O:22])[C:6]=2[CH:23]=1

Participants

3

Reactant 2

HCID 18324905HCID 18324905, compoundHCID 18324986HCID 18324986, compound

Product 1

HCID 9865453HCID 9865453, compound

Procedure

The title compound was prepared from 6-fluoro-3-iodo-2-(4-(methylsulfonyl)phenyl)-4H-1-benzopyran-4-one and lithium trimethoxy-3-pyridinylboronate by the same method as described in Step 5 of Example 1.

Sources & evidence

ORD record
ord-2b91a5fc30e744e6b747c8a2d0349df5
Source dataset
uspto-grants-2002_01
Patent number
US06340694B1

Reaction notes

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