HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 15490844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | HCID 10546822 | HCID 10546822 | — |
| Product | HCID 15490844 | HCID 15490844 | — |
Reaction Steps
9[2-bromo-4(2-propyl)phenyl]-2-methyl-6-chloropurine (1.3 g) and morpholine (10 mL) were combined under nitrogen and refluxed for 6 hrs. The reaction mixture was concentrated by rotovap and the residue was purified by flash chromatography (CH2C2:MeOH, 50:1; silica) to yield a yellow solid (0.54 g). MS (M+H)+416, 418.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342503B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-befd2aa509934687811fd9f61c1190c6 |
| Source note | uspto-grants-2002_01 |