HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 86757754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Dimethyl Sulfoxide | HCID 679 | — |
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | HCID 577984 | HCID 577984 | — |
| Reactant | 6,6'-Diazenediyldi(1,2,4,5-tetrazin-3-amine) | HCID 71361314 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86757754 | HCID 86757754 | — |
Reaction Steps
The present invention further includes a process of preparing 3,3′-azobis(6-amino-1,2,4,5-tetrazine) including reacting 3,6-bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine with hydrazine to form a first intermediate product, reacting said first intermediate product with N-bromosuccinimide in acetonitrile to form a second intermediate product, reacting said second intermediate product with ammonia in DMSO to form a 3,3′-azobis(6-amino-1,2,4,5-tetrazine) DMSO solvate, and converting said 3,3′-azobis(6-amino-1,2,4,5-tetrazine) DMSO solvate to 3,3′-azobis(6-amino-1,2,4,5-tetrazine).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342589B1 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-ab6f6a75f4f442288ced3841f3233535 |
| Source note | uspto-grants-2002_01 |