Kasugamycin hydrochloride → An inositol

Participants

Reaction Conditions

Reaction Steps

Kasugamycin hydrochloride (1 g), 5 mL deionized H2O and Diaion™ SK 116 resin (6 g) were combined and heated 4 h at 85° C., and then at 100° C. for 3 h. The catalyst was removed by filtration through a course scintered glass funnel and washed with deionized H2O (20 mL). The mixture was purified as above, using ion exchange resins and charcoal, yielding D-chiro-inositol (15%).

Provenance & Evidence