HuagongsheHuagongshe Chemistry Print Report · For research reference only
4,5-Dibromothiophene-2-sulfonyl chloride → HCID 15342059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4,5-Dibromothiophene-2-sulfonyl chloride | HCID 522755 | — |
| Reactant | 4-Bromo-3-methylisoxazol-5-amine | HCID 10487519 | — |
| Product | HCID 15342059 | HCID 15342059 | 45% |
Reaction Steps
N-(4-bromo-3-methyl-5-isoxazolyl)-4,5-dibromothiophene-2-sulfonamide was prepared in the same manner as described in Example 2 from 5-amino-4-bromo-3-methylisoxazole and 4,5-dibromothiophene-2-sulphonyl chloride in 45% yield. Purification was achieved by recrystallization from ethyl acetate/hexanes to give a crystalline solid, m.p. 153-155° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342610B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-34bba4c5bbb54bf88edfcb6f0c952e28 |
| Source note | uspto-grants-2002_01 |