HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Methoxyphenyl)boronic acid → N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Methoxyphenyl)boronic acid | HCID 2734370 | — |
| Reactant | N-(5-bromothiophenesulfonyl)pyrrole | HCID 23445587 | — |
| Product | N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole | HCID 22998523 | 93% |
Reaction Steps
N-[5-(3-methoxyphenyl)thiophene-2-sulfonyl]pyrrole was prepared in the same manner as described in Example 32C from 3-methoxyphenylboronic acid and N-(5-bromothiophene-2-sulfonyl)pyrrole in 93% yield. This was purified by recrystallization using hexane/ethyl acetate as solvent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06342610B2 |
| Source dataset | uspto-grants-2002_01 |
| ORD ID | ord-10e34ba276f8476db1d32a98a71ccc43 |
| Source note | uspto-grants-2002_01 |