反应详情

This material was prepared by heating 2-benzylthio-5-(2,2,2-trifluoroethoxy)-1,2,4-triazolo[1,5-a]pyrimidine in boiling ethanol. The hot mixture was filtered and the filtrate was concentrated. The crude product was recrystallized from isopropanol to yield the desired product as a solid, m.p. 115°-117° C. IR and 1HNMR spectra were in agreement with the assigned structure.

1. customThis material was prepared
2. filtrationThe hot mixture was filtered
3. concentrationthe filtrate was concentrated
4. customThe crude product was recrystallized from isopropanol