HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10687479, compound → HCID 10708664, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10687479 | HCID 10687479 | — |
| Catalyst | Zinc copper couple | HCID 10290809 | — |
| Product | HCID 10708664 | HCID 10708664 | 32% |
Reaction Steps
This material was prepared in 32% yield by reduction of 2-benzylthio-5,7-dichloro-6-methyl-1,2,4-triazolo[1,5-a]pyrimidine with zinc-copper couple following the general procedure described in Example 21. The desired product was isolated as a solid, m.p. 179°-181° C. IR and 1H NMR spectra were in agreement with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04741764 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-6338019c30b4464cb6032a65791da948 |
| Source note | uspto-grants-1988_05 |