HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1,1-Trifluoro-2,4-pentanedione → HCID 14155097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1,1-Trifluoro-2,4-pentanedione | HCID 73943 | — |
| Reactant | HCID 178509291 | HCID 178509291 | — |
| Product | HCID 14155097 | HCID 14155097 | 84% |
Reaction Steps
This material was prepared in 84% yield from 3-amino-5-benzylthio-1,2,4-triazole and 1,1,1-trifluoro-2,4-pentanedione following the general procedure described in Example 34. The product was purified by recrystallization from benzene-hexane to yield a tan solid, m.p. 83.5°-84.5° C. IR, 1H NMR and 19F NMR spectra were in agreement with the assigned structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04741764 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-ffcc0e06e4d34a45aefaa5ae961d01d5 |
| Source note | uspto-grants-1988_05 |