Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | 2,4-Dimethylphenol | HCID 7771 | — |
| Product | HCID 20026257 | HCID 20026257 | — |
Reaction Steps
To a 13 g aqueous solution (33%) of polyethyleneimine CORCAT 150 (from Cordova Chemical Company) containing 0.1 mole of available amine nitrogen is added 10.8 g of 2,4-dimethyl phenol (0.1 mole). The solution is maintained below 20° C., while a 37% aqueous formaldehyde solution (0.11 mole) is added slowly with stirring. The solution is allowed to stand for an hour at ambient temperature and then warmed to 80° C. for 2 hrs. The aqueous solution is used without purification in subsequent experiments.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04741831 |
|---|
| Source dataset | uspto-grants-1988_05 |
|---|
| ORD ID | ord-b9f32662225345e484617949432afffc |
|---|
| Source note | uspto-grants-1988_05 |
|---|