Methylhydroxylamine → N-methyl nonanohydroxamic acid

HRID 1252015Notes

Reaction equation

[CH3:1][NH:2][OH:3].[C:4](Cl)(=[O:13])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12].C([N+]([O-])=O)CCCCCCCCC>>[CH3:1][N:2]([C:4](=[O:13])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])[OH:3]

Participants

Reactant 3

HCID 11647Methylhydroxylamine

HCID 69819Nonanoyl chloride

HCID 2206471-Nitrodecane

Product 1

HCID 14205292N-methyl nonanohydroxamic acid

Procedure

The starting N-methyl nonanohydroxamic acid was prepared by acylation of methyl hydroxylamine with nonanoyl chloride and was a white, waxy solid, M.P. 29° C., represented by the formula C10H21NO2.

Sources & evidence

ORD record: ord-e26867d5007d41619e4c3dcc3cfd4910
Source dataset: uspto-grants-1988_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04741887

Reaction notes

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