HRID1252031

反应详情

EQUATION

反应方程式

HRID 1252031 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

6.5 g of N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolamine obtained in Example 1 was hydrogenated in the presence of a catalyst composed of palladium on carbon in 40 ml of ethanol. The ethanol layer was then separated from the catalyst and the solvent was distilled off to afford 6.7 g (yield 94%) of the title compound as a colorless oil.

WORKUP

后处理

  1. customThe ethanol layer was then separated from the catalyst
  2. distillationthe solvent was distilled off