HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Methoxyphenyl)but-3-en-2-one → 4-(3-Methoxyphenyl)butan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Methoxyphenyl)but-3-en-2-one | HCID 182007 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 4-(3-Methoxyphenyl)butan-2-one | HCID 11423902 | 99.2% |
Reaction Steps
A solution of 30.1 g of 4-(3-methoxyphenyl)-3-buten-2-one in 200 ml of MeOH was hydrogenated over 200 mg of 10% palladium on carbon for two hours. The catalyst was filtered and the solvent evaporated in vacuo to give 30.2 g of yellow oily 4-(3-methoxyphenyl)-2-butanone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04742084 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-554dee67ee5f4a57ba51d74a232133c6 |
| Source note | uspto-grants-1988_05 |