Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Cyclohexylamine | HCID 7965 | — |
| Reactant | HCID 53956536 | HCID 53956536 | — |
| Product | HCID 178440548 | HCID 178440548 | 58.2% |
Reaction Steps
A mixture of 20 g of allylmethylbicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic anhydride and 9.09 g of cyclohexylamine is heated at 135° C. for 3 hours, and the product is then distilled in vacuo. 16 g of a yellow, viscous oil distill over between 128° and 138° C. at 2.5 Pa, corresponding to a yield of 58.2%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04742166 |
|---|
| Source dataset | uspto-grants-1988_05 |
|---|
| ORD ID | ord-16f22498ef1b4c33a313cc09d7804112 |
|---|
| Source note | uspto-grants-1988_05 |
|---|
