Hydrazine → HCID 85560040, compound

HRID 1252372Notes

Reaction equation

HRID 1252372 reaction equation
[CH3:1][C:2]1[NH:6][C:5]([C:7]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[CH:10]=[CH:9][CH:8]=2)=[N:4][C:3]=1[C:17]([O:19]CC)=O.[NH2:22][NH2:23]>>[CH3:1][C:2]1[NH:6][C:5]([C:7]2[C:16]3[C:11](=[CH:12][CH:13]=[CH:14][CH:15]=3)[CH:10]=[CH:9][CH:8]=2)=[N:4][C:3]=1[C:17]([NH:22][NH2:23])=[O:19]

Participants

3

Reactant 2

HCID 9321HydrazineHCID 53404405Ethyl 4-methyl-2-(naphthalen-1-yl)-1H-imidazole-5-carboxylate

Product 1

HCID 85560040HCID 85560040, compound

Procedure

A mixture of 5.0 g of the above ester and 25 ml of hydrazine was refluxed overnight and then cooled. The solid was collected, stirred with water and cooled. The solid was collected, giving 4.5 g of 5-methyl-2-(1-naphthalenyl)-1H-imidazole-4-carboxylic acid, hydrazide.

Workup

  1. temperaturewas refluxed overnight
  2. temperaturecooled
  3. customThe solid was collected
  4. temperaturecooled
  5. customThe solid was collected

Sources & evidence

ORD record
ord-3ce6cf2706674dffa22d3ae111bf8bf4
Source dataset
uspto-grants-1988_05
Patent number
US04743586

Reaction notes

Loading…