4-Chlorophthalic anhydride → HCID 20140094, compound
Reaction equation
[Cl:1][C:2]1[CH:12]=[C:6]2[C:7]([O:9][C:10](=[O:11])[C:5]2=[CH:4][CH:3]=1)=[O:8].[N:13]1[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][CH2:20][CH2:21][CH2:22][NH2:23])[CH:14]=1>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:10]([OH:9])=[O:11])=[C:6]([C:7]([NH:23][CH2:22][CH2:21][CH2:20][CH2:19][C:15]2[CH:14]=[N:13][CH:18]=[CH:17][CH:16]=2)=[O:8])[CH:12]=1Participants
3
Procedure
When 5-chlorophthalic anhydride was reacted with 4-(3-pyridinyl)butylamine by the procedure of Example 12, the above compound, mp 152°-154° C. was obtained.
Workup
- customthe above compound, mp 152°-154° C. was obtained
Sources & evidence
- ORD record
- ord-693eeee255c14a38bbcc34d08b2ed4d5
- Source dataset
- uspto-grants-1988_05
- Patent number
- US04743610
Reaction notes
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