Bromine → HCID 86117534, compound

HRID 1252792Notes

Reaction equation

HRID 1252792 reaction equation
[CH2:1]([N:8]([CH2:14][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[CH:9]1[CH2:12][CH2:11][C:10]1=[O:13])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Br:21]Br>C(Cl)(Cl)Cl>[BrH:21].[CH2:14]([N:8]([CH2:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1)[CH:9]1[CH2:12][CH:11]([Br:21])[C:10]1=[O:13])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Participants

4

Reactant 2

HCID 24408BromineHCID 19850278HCID 19850278, compound

Product 1

HCID 86117534HCID 86117534, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent2×

Procedure

2-(Dibenzylamino)cyclobutanone is dissolved in CHCl3 (1 molar conc.) and treated dropwise with one equivalent of bromine dissolved in CHCl3 (1 molar conc.) at 0° C. After stirring the mixture for 30 minutes, evaporate the solution to obtain the desired product of this step.

Workup

  1. customevaporate the solution

Sources & evidence

ORD record
ord-729a3d6cc32045fe91f19cc7b33dc2f9
Source dataset
uspto-grants-1988_05
Patent number
US04745222

Reaction notes

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