HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 53687305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | HCID 53833353 | HCID 53833353 | — |
| Catalyst | Acetic Acid | HCID 176 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53687305 | HCID 53687305 | — |
Reaction Steps
N-(2-Benzoylthioacetyl)-L-proline obtained in Example 29, step (a) is dissolved in methanol and an ethereal solution of diazomethane is added until there is a persistent yellow color. After 15 minutes, a few drops of acetic acid are added and the solvent is removed in vacuo to obtain N-(2-benzoylthioacetyl)-L-proline methyl ester.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04745124 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-dbb7b5475f75409f9599fcbc6a7ca49b |
| Source note | uspto-grants-1988_05 |