HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 20130640, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 54392110 | HCID 54392110 | — |
| Solvent | Isopropanol dimethylformamide | HCID 20197112 | — |
| Product | HCID 20130640 | HCID 20130640 | — |
Reaction Steps
using isopropyl 2-chloro-4-fluoro-5-{3-[2-(ethoxycarbonyl)-1-ethyl-1-propenyl]ureido}-benzoate with sodium isopropylate in an isopropanol/dimethylformamide mixture there is obtained isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-4-ethyl-5-methyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate, m.p. 192°-194° C.,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746352 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-0f69368096f0449391c4809158526597 |
| Source note | uspto-grants-1988_05 |