HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 20130676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 20130579 | HCID 20130579 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 20130676 | HCID 20130676 | — |
Reaction Steps
using isopropyl 2-bromo-4-fluoro-5-(1,2,4,5,6,7-hexahydro-2,4-dioxo-3H-cyclopenta[d]pyrimidin-3-yl)-benzoate and dimethyl sulphate with sodium isopropylate in isopropanol there is obtained isopropyl 2-bromo-4-fluoro-5-(1,2,4,5,6,7-hexahydro-1-methyl-2,4-dioxo-3H-cyclopenta-[d]pyrimidin-3-yl)-benzoate, m.p. 116°-120° C.,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746352 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-9d6291d83146409d8a23934bf0db3f60 |
| Source note | uspto-grants-1988_05 |