HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 20130668, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 20130618 | HCID 20130618 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 20130668 | HCID 20130668 | — |
Reaction Steps
using isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-5-fluoro-4-fluoromethyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate and dimethyl sulphate in dimethylformamide there is obtained isopropyl 2-chloro-4-fluoro-5-[3,6-dihydro-5-fluoro-4-fluoromethyl-3-methyl-2,6-dioxo-1(2H)-pyrimidinyl]-benzoate, m.p. 85°-89° C.,
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746352 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-1c86319101d14469839893bc5d90aed2 |
| Source note | uspto-grants-1988_05 |