HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine → Accelerator DM
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine | HCID 807 | — |
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178418395 | HCID 178418395 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | Accelerator DM | HCID 8447 | — |
Reaction Steps
A solution of 20 g of iodine and 115 g of potassium iodide in 400 ml of water is added dropwise to a solution of 30 g of 2-mercapto-benzothiazole and 1.6 g of sodium hydroxide in 800 ml of absolute ethanol. After completion of the addition, the mixture is stirred for 30 minutes at ambient temperature and the precipitate is then filtered off, washed with ethanol and then washed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746654 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-9d4a1d8900cd4aadac58c5223159e0e2 |
| Source note | uspto-grants-1988_05 |