HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20137892, compound → HCID 20137884, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20137892 | HCID 20137892 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 20137884 | HCID 20137884 | — |
Reaction Steps
A solution of 200 mg of 4-(α-phosphonoacetamido)-picolinic acid in 50 ml of water is hydrogenated over 1.0 g of platinum oxide at 3 atmospheres pressure for 8 hours. After filtration and evaporation to dryness the residue is triturated with ethanol to afford 4-(α-phosphonoacetamido)-piperidine-2-carboxylic acid as a mixture of cis and trans isomers.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746653 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-e55ed2ea1ba04f5dbcee60225b84b931 |
| Source note | uspto-grants-1988_05 |