HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 13055728, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | 1,3-Dibromopropane | HCID 8001 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-Hydroxy-3,4-dihydro-2(1H)-quinolinone | HCID 2774040 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 13055728 | HCID 13055728 | — |
Reaction Steps
A mixture of 12.6 g (0.076 mol) of 6-hydroxy-1,2,3,4-tetrahydro-2-quinolinone, 15.8 g (0.115 mol) of potassium carbonate (anhydrous and powdered), 46.5 g (0.23 mol) of 1,3-dibromopropane and 40 ml of N,N-dimethylformamide is stirred at room temperature for 20 hours. 200 ml of water and 100 ml of petroleum ether are added and, after stirring for 1 hour, the precipitate which has formed is filtered off with suction, washed with petroleum ether and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04746661 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-aeb31252e9404d748858c580644f4b19 |
| Source note | uspto-grants-1988_05 |