Ammonia → 4-(2-Aminopropan-2-yl)phenol
Reaktionsgleichung
[CH3:1][C:2]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1)=[CH2:3].[NH3:11]>>[NH2:11][C:2]([C:4]1[CH:9]=[CH:8][C:7]([OH:10])=[CH:6][CH:5]=1)([CH3:1])[CH3:3]Komponenten
3
Versuchsvorschrift
A 0.10-g sample of 4-(1-methylethenyl)phenol is exposed to excess, gaseous ammonia for about 1 day at 50° C. under autogenous pressure in a closed heavy wall glass bottle. The excess ammonia is purged and a quantitative yield of 2-amino-2-(4-hydroxyphenyl)propane is obtained.
Aufarbeitung
- customfor about 1 day
- customat 50° C.
- customThe excess ammonia is purged
Quellen und Nachweise
- ORD-Eintrag
- ord-dfd9ab03932f47fbae7712d9e63a28d9
- Quelldatensatz
- uspto-grants-1988_05
- Patentnummer
- US04746754
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