Methyl isothiocyanate → HCID 54138282, compound

Participants

Reaction Steps

A solution of 5-(4-amino-1,2,3-triazol-2-yl)valeronitrile (1.65 g.) in acetonitrile (5 ml.) and methylisothiocyanate (0.73 g.) was stirred for 18 hours at ambient temperature and then heated under reflux for 6 hours. The solvent was evaporated and the residue was triturated with ether/EtOH to give 5-[4-(3-methylthioureido)-1,2,3-triazol-2-yl]valeronitrile as a white solid.

Provenance & Evidence