HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → 2-Amino-4-hydroxymethyl-6-methylbenzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | Methyl 2-amino-6-methylbenzothiazole-4-carboxylate | HCID 19894946 | — |
| Product | 2-Amino-4-hydroxymethyl-6-methylbenzothiazole | HCID 19894957 | — |
Reaction Steps
30 g (0.135 mol) of 5a are reduced with 337.7 ml (0.405 mol) of DIBAL (20% strength solution in toluene) in analogy to Example 1a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04748163 |
| Source dataset | uspto-grants-1988_05 |
| ORD ID | ord-dd914f4122ac45a5bdf0529ed9599ae5 |
| Source note | uspto-grants-1988_05 |