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HRID1253225

反应详情

EQUATION

反应方程式

HRID 1253225 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：CC(C(=O)O)[CH](C)[Ge]([Cl])([Cl])[Cl]
HCID13249025

未命名化合物

PRODUCTS

生成物

1
结构：CC(C(=O)Cl)[CH](C)[Ge]([Cl])([Cl])[Cl]
HCID13249038

2-Methyl-3-(trichlorogermyl)butanoyl chloride

C5H8Cl4GeO

收率 90.4%

PROCEDURE

实验过程

28.0 g (0.1 mol) of 2-methyl-3-(trichlorogermyl)butanoic acid was treated with 100 ml of thionyl chloride and then distilled under reduced pressure to obtain 27.0 g (yield: 90.4%) of 2-methyl-3-(trichlorogermyl)-butanoyl chloride as a light yellow fraction having a boiling point of 99° to 100° C./6 mmHg.

WORKUP

后处理

  1. distillationdistilled under reduced pressure