HCID 15611127, compound → HCID 15611128, compound

Participants

Reaction Steps

A mixture of 4.8 g of Ethyl 2-(2-n-propyl-3-hydroxy-4-acetylphenoxy)-2-(3,4-dichlorophenyl)acetate in 100 ml of dioxane and 15 ml of concentrated hydrochloric acid was refluxed for 70 hours. The reaction mixture was then cooled, concentrated in vacuum to give 2.9 g of the crude solid, which was crystallized from hexane to give 1.8 g of pure product, melting point 177°-180° C.

Provenance & Evidence