HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → Acetyltriphenylene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Triphenylene | HCID 9170 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Acetyltriphenylene | HCID 86641842 | 97% |
Reaction Steps
Triphenylene (1 equivalent) is reacted at 0° C. with 2.1 equivalents of AlCl3 and 21.0 equivalents of CH3COCl in CH2Cl2. After stirring at room temp. for 3 hours, the reaction product (acetyltriphenylene) was obtained in 97% yield, and is used in step b).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08455112B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-50762937bfe84de5b8de680d0acea52e |
| Source note | uspto-grants-2013_06 |