HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → N-(2-hydroxyethyl)-9-octadecenyl succinimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | Dihydro-3-(1-octadecen-1-yl)-2,5-furandione | HCID 225771 | — |
| Product | N-(2-hydroxyethyl)-9-octadecenyl succinimide | HCID 68776476 | 75.3% |
Reaction Steps
A 50 mL reaction flask was charged with 35.1 g of octadecenyl succinic anhydride (manufactured by Tokyo Chemical Industry Co., Ltd.) and 6.1 g of ethanolamine (manufactured by Tokyo Chemical Industry Co., Ltd.), and the resulting mixture was reacted at 110° C. for 6 hours under continuous nitrogen purging and with vigorous stirring. The reaction product was purified by silica gel column chromatography (mobile phase: ethyl acetate/hexane), yielding 29.6 g of N-(2-hydroxyethyl)-9-octadecenyl succinimide (yield: 75.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08455413B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-9b56a159bc26419691df952b38a2e249 |
| Source note | uspto-grants-2013_06 |