2-(Cyclohex-1-en-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane → 3-Cyclohex-1-enyl-5-nitro-2-(2,2,2-trifluoro-ethoxy)-pyridine

Participants

Reaction Steps

This compound was prepared following the same procedure as described for Example 1b using 3-bromo-5-nitro-2-(2,2,2-trifluoro-ethoxy)-pyridine (Example 1a, 1 g, 3.18 mmol) and 2-(1-cyclohexen-1-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane (CAN 141091-37-4, 0.73 g, 3.5 mmol) as starting materials. The title compound (520 mg, 54.0%) was isolated as off white solid; NMR complies.

Provenance & Evidence