4-Bromo-3,5-dimethylphenol → 4-(4-Bromo-3,5-dimethylphenoxy)-2-methylbutan-2-ol

HRID 1253803Notes

Reaction equation

HRID 1253803 reaction equation
CC1C=CC(S(O[CH2:12][CH2:13][C:14]([OH:17])([CH3:16])[CH3:15])(=O)=O)=CC=1.[Br:18][C:19]1[C:24]([CH3:25])=[CH:23][C:22]([OH:26])=[CH:21][C:20]=1[CH3:27]>>[Br:18][C:19]1[C:24]([CH3:25])=[CH:23][C:22]([O:26][CH2:12][CH2:13][C:14]([CH3:16])([OH:17])[CH3:15])=[CH:21][C:20]=1[CH3:27]

Participants

3

Reactant 2

HCID 819704-Bromo-3,5-dimethylphenolHCID 140012952-Methyl-4-[(4-methylbenzenesulfonyl)oxy]butan-2-ol

Product 1

HCID 679729214-(4-Bromo-3,5-dimethylphenoxy)-2-methylbutan-2-olYield 0.1%

Procedure

According to the method of (Example 36) <Step 1>, from 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate (5.1 g) and 4-bromo-3,5-dimethylphenol (3.6 g), the subject compound (5.2 mg) was obtained as a colorless oil.

Sources & evidence

ORD record
ord-97861cdbba264fa08a02ab3beb1a0df5
Source dataset
uspto-grants-2013_06
Patent number
US08455500B2

Reaction notes

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