2-Methyl-4-[(4-methylbenzenesulfonyl)oxy]butan-2-ol → HCID 59544297, compound

HRID 1253807Notes

Reaction equation

HRID 1253807 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]([CH3:10])[C:5]([OH:9])=[N:6][C:7]=1[CH3:8].CC1C=CC(S(O[CH2:22][CH2:23][C:24]([OH:27])([CH3:26])[CH3:25])(=O)=O)=CC=1>>[Br:1][C:2]1[CH:3]=[C:4]([CH3:10])[C:5]([O:9][CH2:22][CH2:23][C:24]([CH3:26])([OH:27])[CH3:25])=[N:6][C:7]=1[CH3:8]

Participants

3

Reactant 2

HCID 140012952-Methyl-4-[(4-methylbenzenesulfonyl)oxy]butan-2-olHCID 178422450HCID 178422450, compound

Product 1

HCID 59544297HCID 59544297, compoundYield 75.8%

Procedure

According to the method of (Example 36) <Step 1>, from 5-bromo-3,6-dimethylpyridin-2-ol (0.74 g) and 3-hydroxy-3-methylbutyl 4-methylbenzenesulfonate (1.0 g), the subject compound (0.80 g) was obtained as a white solid.

Sources & evidence

ORD record
ord-51a27112b4784313a05662809ce89109
Source dataset
uspto-grants-2013_06
Patent number
US08455500B2

Reaction notes

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